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Wolfgang Holzbach

Ruhr University Bochum

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Zeitschrift für Naturforschung B | 1982

η2-Koordination eines Hydroxylamid(2-)Anions: Die Kristallstruktur von [Mo(NO)(terpy)(CN)(HNO)] 2H2O / η2-Coordination of a Hydroxylamido(2-) Anion: The Crystal Structure of [Mo(NO)(terpy)(CN)(HNO)]2H2O

Karl Wieghardt; Wolfgang Holzbach; Johannes Weiss

Abstract The red, diamagnetic complex [Mo(NO)(terpy)(CN)(HNO)] • 2H2O crystallizes in the triclinic space group P1̅(C1i-No2) with cell constants a = 867.1(3), b = 1008.4(4), c = 1095.6(3) pm, a = 73.64(3)°, β = 83.54(3)°, γ = 83.16(3)°, and Z = 2. The final R value of the single crystal X-ray analysis is 0.063 for 1922 unique reflections. The structure consists of neutral complexes of [Mo(NO)(terpy)(CN)(HNO)]. The geometry about the molybdenum is a distorted pentagonal bipyramid with a linear NO and CN group in the axial positions, a triclentate terpyridine ligand and an O,N-coordinated HNO2- ligand in equatorial positions.

Chemische Berichte | 1980

Reaktionen von Hydroxylamin mit Molybdän(VI): Synthese von (Hydroxylamido-O,N)nitrosylmolybdän-Komplexen. Die Struktur des [(Hydroxylamido-O,N)nitrosylbis(1,10-phenanthrolin)molybdän]-Kations

Karl Wieghardt; Wolfgang Holzbach; Bernhard Nuber; Johannes Weiss

Angewandte Chemie | 1979

Reactions of Molybdate(VI) with Hydroxylamine and N‐Methylhydroxylamine

Karl Wieghardt; Wolfgang Holzbach; Johannes Weiss; Bernhard Nuber; Boris Prikner

Inorganic Chemistry | 1980

Complexes of (hydroxylamido-O,N)molybdenum(VI). Preparation and crystal structures of [MoO(H(CH3)NO)2(HNC(S)N(CH3)O)] and [MoO(H(CH3)NO)(HNC(S)N(CH3)O)(H2NC(S)N(CH3)O)].H2O

Karl Wieghardt; Edgar Hofer; Wolfgang Holzbach; Bernhard Nuber; Johannes Weiss

Angewandte Chemie | 1979

Reaktionen von Molybdat(VI) mit Hydroxylamin und N‐Methylhydroxylamin

Karl Wieghardt; Wolfgang Holzbach; Johannes Weiss; Bernhard Nuber; Boris Prikner

Chemische Berichte | 1981

Synthesen mit (Hydroxylamido(1–)–O,N)molybdän(VI)‐Komplexen und Alkylcyaniden. Die Strukturen von Bis(N‐hydroxy‐Nmethylacetamidinato(1–)‐O,N′)(N‐methyl‐hydroxylamido(1–)‐O,N)oxomolybdän(VI)‐perchlorat und von μ‐Oxo‐bis[N‐hydroxy‐N‐methylacetamidinato(1–)‐O, N′→ Mo1;O → Mo2‐cis‐dioxo]dimolybdän(VI)

K. Wieghardt; Wolfgang Holzbach; Edgar Hofer; Johannes Weiss

Inorganic Chemistry | 1981

Reactions of hydroxylamido-(O,N) complexes of vanadium(V) and of molybdenum(VI) with oxalic acid. Crystal structure of (Et2NHOH)2[Mo2O4(Et2NO)2(C2O4)2]: a .mu.-dioxo complex containing two pentagonal-bipyramidal molybdenum(VI) ions

Karl Wieghardt; Wolfgang Holzbach; Johannes Weiss

Angewandte Chemie | 1979

Synthese eines Hydroxylamido(2 – )‐O, N‐(nitrosyl)‐molybdän‐Komplexes

Karl Wieghardt; Wolfgang Holzbach

Angewandte Chemie | 1981

Configurational Isomerization of N,N-Disubstituted Hydroxylamido(1-)-O,N-Molybdenum(VI) Complexes†

Edgar Hofer; Wolfgang Holzbach; Karl Wieghardt

Angewandte Chemie | 1981

Konfigurationsisomerisierung an N,N‐disubstituierten Hydroxylamido(1‐)‐O,N‐molybdän(VI)‐Komplexen

Edgar Hofer; Wolfgang Holzbach; Karl Wieghardt

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Johannes Weiss

Heidelberg University

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Karl Wieghardt

Max Planck Society

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K. Wieghardt

Ruhr University Bochum

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Bernhard Nuber

Heidelberg University

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Boris Prikner

Heidelberg University

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W. Swiridoff

Heidelberg University

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