Z. Ranachowski

Acoustic investigations of long-rod insulators and their material properties

The paper presents a nondestructive ultrasonic method of investigating long-rod insulators used on overhead power lines and in substations. A correlation between the degree of degradation of porcelain C 120 and the ultrasonic wave propagation and attenuation parameters was established. The ultrasonic method was used to analyze the quality of groups of line and post insulators after many years of service. Also a new mechanoacoustic method of investigating the stages in the degradation of insulator porcelain was applied. As a result of the investigations carried out on samples of porcelain C 130 the successive stages in the degradation of ceramic insulators during their service life were determined.

Analysis of acoustic emission signals at austempering of steels using neural networks

Bearing steel 100CrMnSi6-4 and tool steel C105U were used to carry out this research with the steels being austempered to obtain a martensitic-bainitic structure. During the process quite a large number of acoustic emissions (AE) were observed. These signals were then analysed using neural networks resulting in the identification of three groups of events of: high, medium and low energy and in addition their spectral characteristics were plotted. The results were presented in the form of diagrams of AE incidence as a function of time. It was demonstrated that complex transformations of austenite into martensite and bainite occurred when austempering bearing steel at 160 °C and tool steel at 130 °C respectively. The selected temperatures of isothermal quenching of the tested steels were within the area near to MS temperature, which affected the complex course of phase transition. The high activity of AE is a typical occurrence for martensitic transformation and this is the transformation mechanism that induces the generation of AE signals of higher energy in the first stage of transition. In the second stage of transformation, the initially nucleated martensite accelerates the occurrence of the next bainitic transformation.

Mechanoacoustic research method of degradation processes in electroceramics materials

The paper presents the concept of mechanoacoustic testing of degradation processes of ceramic materials, which is applied to diagnose high voltage insulators in operation. The method depends on the application of slowly increasing compressive loading acting on the sample, with simultaneous recording of acoustic emission (AE) descriptors. The process of loading is continued to the destruction or stopped at different stresses, and the samples are subjected to microscopic examination. Microscopic analysis of the samples enables determining the effects of stress action. The results were compared with the images of similar materials obtained from the insulators after different periods of operation. On this basis, there were distinguished consecutive stages of ageing of electrotechnical porcelain materials and corresponding effects of their structure degradation. Using slowly increasing quasi-static compressive loading in a relatively short-term mechanoacoustic test makes it possible to get results similar to those of long lasting degradation effects in operated electroinsulating objects. Using this method there is possible to describe the factors which affect short and long-term mechanical strength of the tested materials. There is also possible assessment of the validity and application of the theories explaining the strength of porcelains. There was presented research of the influence of the mullite phase on the short- and long-term mechanical strength of electrotechnical porcelain of different types.

Effect of Microstructure on Rolling Contact Fatigue of Bearings

There has been proposed an innovative thermal treatment of bearing steel 100CrMnSi6-4, where the existing standard heat treatment has been replaced by austempering. The structure of low-temperature tempered martensite has been replaced by a microstructure composed of martensite and lower bainite with midrib. The kinetics of bainitic transformation and isothermal martensitic transition at selected austempering temperatures was controlled by acoustic emission. The research on contact strength was made under the conditions of rolling-sliding friction. The microstructure was revealed with the use of a light microscope and the forms of pitting wear were displayed by a scanning electron microscope. It was found that the optimum microstructure providing the best used contact strength of the tested steel is conditioned by the formation of a lower bainite with midrib at the temperatures near MS. A plausible cause of the increased resistance to pitting is bifurcation of fatigue cracks on dispersion bainitic carbides in combination with primary carbides, in bainitic-martensitic matrix.

Microhardness testing procedure applied to blended cement based matrix

In the paper a new method of determination of cement paste microhardeness is presented. It includes the procedure of systematic indentation with a Vickers tip and a statistical processing of population of obtained results. The tested specimens were cast with different kinds of blended cements, containing high calcium fly ash (HCFA) as one of major components. Differences in values of microhardeness obtained for six series of tested specimens mixes are discussed and compared with compressive strength of investigated materials.

Saffil alumina fibers reinforced dual-phase Mg-Li and Mg-Li-Zn alloys

The gas pressure infiltration technique was used to prepare Saffil alumina fibers reinforced Mg-Li and Mg-Li-Zn matrix composites with a dual-phase matrix structure. There was investigated the effect of variable Li content (6.2–10.3 wt.% Li) and Zn alloying (∼ 1.5 wt.% Zn) on the proof stress Rp0.2 of prepared composites. Rp0.2 values increased monotonously with rising fraction of Saffil fibers (5, 10 and 15 vol.%) reaching the maximum of about 250 MPa for Mg-Li matrix composites. Rp0.2 values of Mg-Li-Zn matrix composites were lower. Strengthening effect of Saffil fibers was promoted by the displacement redox reaction with Mg-Li and Mg-Li-Zn melts in which only Li significantly participated. Zn alloying retarded the displacement redox reaction. Too extensive reaction, however, resulted in the fiber damage and the drop in composite strength. K e y w o r d s: Mg-Li alloys, Saffil fibers, metal matrix composites, short-fiber strengthening, reactive wetting, displacement reactions

Relation between the plastic instability and fracture of tensile tested Cu-Sn alloys investigated with the application of acoustic emission technique

The work concerns the application of the acoustic emission (AE) method in testing the mechanical properties of continuously cast industrial tin bronze CuSn6P, which reveals tendencies to instable plastic flow connected particularly with the Portevin-Le Chatelier (PLC) effect. The relations between the jerky flow connected with the PLC effect, AE intensity and the evolution of a fracture of the investigated alloy subjected to the tensile test at a strain rate (?? ) of about 1.2·10-3s-1 in the range of temperatures (20÷400?C) has been analyzed. It has been found that the highest intensity of the oscillation of stresses, corresponding to the instability of plastic deformation PLC occurred at 200?C, whereas the maximum of the AE activity is at about 200÷250?C. The brittle intergranular fracture starts in the range of equicohersive temperature (TE) of about 200?C. Plastic deformation of the investigated alloy in the range of the temperature of minimum plasticity, amounting to about 400?C, results in intercrystalline fractures on the entire surface of the stretched samples.

Mechanisms of plastic instability and fracture of compressed and tensile tested Mg-Li alloys investigated using the acoustic emission method

The results of the investigation of both mechanical and acoustic emission (AE) behaviors of Mg4Li5Al alloy subjected to compression and tensile tests at room temperature are compared with the test results obtained using the same alloy and loading scheme but at elevated temperatures. The main aim of the paper is to investigate, to determine and to explain the possible influence of factors related with enhanced internal stresses such as: segregation of precipitates along grain boundaries or solute atoms along dislocations (Cottrell atmospheres) or dislocation pile-ups at grain boundaries which create very high stress concentration leading to fracture. The results show that the plastic instabilities are related to the Portevin–Le Châtelier phenomenon (PL effect) and they are correlated with the generation of AE peaks. The fractography of breaking samples was analyzed on the basis of light (optical), TEM and SEM images.

Mechanical-Acoustic and Structural Study of Degradation Processes in Corundum Ceramics and Aluminous Porcelain

This paper comprises the results of acoustic emission (AE), microscopic and ultrasonic measurements of samples subjected to slowly increasing compressive stress. On the basis of conducted measurements the successive stages of the materials structural degradation have been recognized. The object of study were samples made of C 799 corundum ceramics and C 130 aluminous porcelain. Both investigated materials have at present wide application in the fabrication of numerous technical elements e.g. overhead power line insulators. In case of such objects not only high mechanical strength but especially elevated durability as well as operational reliability are required. Expected “life time” of net insulators during exploitation is about 40 years.