Zhang Xue Yu

Study on a Structure of 2,6-pyridine-dicarboxylic Acid Cobalt Calcium Hexahydrate

The complex C28H32CaCoN4O24 has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Co atom is six-coordinated by two N atoms, four O atoms from two 2,6-pyridinedicarboxylic acid. The Ca atom is eight-coordinated by two N atoms, six O atoms from two 2,6-pyridinedicarboxylic acid and two water molecular. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Study on a Novel Structure of Yttrium Complex, C4H10O10Y

The Y complex C4H10O10Y has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Y atom is coordinated by nine O atoms. The molecular structure stabilized by the O-H…O hydrogen-bonding interactions.

Crystal Structure of Ytterbium Chloride Phenanthroline: [YbCl4]·[C12H8N2]·(H2O)

A novel ytterbium chloride phenanthroline [YbCl4]·[C12H8N2]·(H2O) has been synthesized from a single solution reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Yb atom is coordinated by six Cl atoms. The plane quadrilateral is formed by two Cl2 and two Yb atoms. Molecules form O—H…Cl , O—H…O , O—H…N intramolecular and intermolecular hydrogen bonds and stabilized the molecular structure.

Study on a Novel Structure of Zn Phenanthroline Malic Acid Hydrate, [Zn (C12H8N2)(C4H4O5)(H2O)](H2O)

A novel Zn complex [Zn (C12H8N2)(C4H4O5)(H2O)](H2O) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Zn atom is six-coordinated by two phenanthroline N atoms, three O atoms from malic acid anion and one O atom from water. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Study on a Structure of 2,6-Pyridine-Dicarboxylic Acid Lead, Pb(C7H3NO4)

A novel Pb metal complex Pb(C7H3NO4) has been synthesized from a solution reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Pb atom is seven-coordinated by one N atom and six O atoms. The crystal packing is stabilized by O-H...O and O-H...N hydrogen bonding interactions.

Study on a Structure of 2,6-Pyridine-Dicarboxylic Acid Mn, Mn2(C7H3NO4)24H2O

A novel Mn metal complex C14H14Mn2N2O12 has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Mn atom is six-coordinated by one N atom and four O atoms. The Mn-Mn bond is existent. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Crystal Structure of bi(1,10-phenanthroline)- copper-Cl chlorine hydrate, [CuCl(C12H8N2)2]Cl0.5(H2O)5.5

A novel Cu metal complex [CuCl(C12H8N2)2]Cl 0.5(H2O)5.5 has been synthesized from a solution reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. [CuCl(C12H8N2)2]Cl 0.5(H2O)5.5, Monoclinic, C2/c. a=23.086(2)Å, b =30.090(3)Å, c=7.4580(8)Å, α=γ=90, β=97.67, V=5134.3Å3, Z=8, R1 =0.0923, wR2 =0.2182, T=298K. The crystal packing is stabilized by O-H...O and O-H...Cl hydrogen bonding and Л-Л interactions.

Di(1,10-phenanthroline)-Cobalt(II) Nitrate Iodate Dihydrate, Co(C12H8N2)2NO3I(H2O)2

A novel Co complex Co (C12H8N2)2NO3I(H2O)2 has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Co atom is coordinated with four N atoms from two 1,10-phenanthroline and two O atoms from NO3-, presenting a distorted octahedron geometry. The crystal structure is stabilized by intermolecular O-H...O and O-H...I hydrogen bonds interaction.