Arnaud Jérôme

EUVI: the STEREO-SECCHI extreme ultraviolet imager

The Extreme Ultraviolet Imager (EUVI) is part of the SECCHI instrument suite currently being developed for the NASA STEREO mission. Identical EUVI telescopes on the two STEREO spacecraft will study the structure and evolution of the solar corona in three dimensions, and specifically focus on the initiation and early evolution of coronal mass ejections (CMEs). The EUVI telescope is being developed at the Lockheed Martin Solar and Astrophysics Lab. The SECCHI investigation is led by the Naval Research Lab. The EUVI’s 2048 x 2048 pixel detectors have a field of view out to 1.7 solar radii, and observe in four spectral channels that span the 0.1 to 20 MK temperature range. In addition to its view from two vantage points, the EUVI will provide a substantial improvement in image resolution and image cadence over its predecessor SOHO-EIT, while complying with the more restricted mass, power, and volume allocations on the STEREO mission.

Study of normal incidence of three-component multilayer mirrors in the range 20-40 nm.

We study theoretically and experimentally the increase of normal incidence reflectivity generated by addition of a third material in the period of a standard periodic multilayer, for wavelengths in the range 20 to 40 nm. The nature and thickness of the three materials has been optimized to provide the best enhancement of reflectivity. Theoretical reflectivity of an optimized B4C/Mo/Si multilayer reaches 42% at 32 nm. B4C/Mo/Si multilayers have been deposited with a magnetron sputtering system and a reflectivity of 34% at 32 nm has been measured on a synchrotron radiation source.

Ion-beam-deposited Mo/Si multilayers for EUV imaging applications in astrophysics

Imaging of the solar corona by selecting Fe IX (λ=17.1nm,), Fe XII (λ=19.5nm), Fe XV (λ=28.4nm) and He II (λ=30.4nm) emission lines with a Ritchey-Chretien telescope requires to coat the optics with multilayers having a high accuracy in their layer thicknesses, a high reflectivity and an optimal bandpass. Multilayers were simulated in order to determine the most adequate formula for each wavelength channel. Mo/Si coatings were deposited by using the ion beam sputtering technique in a high vacuum chamber equipped with a micro balance and an in-situ reflectometer. The multilayers were studied by grazing angle reflectometry at 0.1541nm, and their reflectances around the operating wavelengths were measured on the SA62 IAS/LURE beam line of the SuperACO synchrotron facility located at Orsay. In addition, aging versus time and behavior of the multilayers under a rapid thermal annealing were investigated. Performances of the ion-beam deposited multilayers have been improved compared to the Mo/Si coatings obtained in the past by the e-beam evaporation technique for the SOHO mission Extreme UV Imaging Telescope (EIT). The EUVI telescopes for the STEREO mission are being proceduced by depositing these new generation of multilayers onto primary and secondary mirrors. The reflectivity measurements on a telescope are presented.

HECOR: a HElium CORonagraphy aboard the Herschel sounding rocket

HECOR (HElium CORonagraph) is a coronagraph designed to observe the solar corona at 30.4 nm between 1.2 and 4 solar radii. The instrument is part of the Herschel sounding rocket payload to be flown from White Sands Missile Range in December 2007. Much like for neutral hydrogen, the residual singly ionized helium present in the corona can be detected because it resonantly scatters the intense underlying chromospheric radiation. Combined with the simultaneous measurements of the neutral hydrogen corona made by SCORE, the other coronagraph of the Herschel payload, the HECOR observations will provide novel diagnostics of the solar wind outflow. HECOR is an externally occulted coronagraph of very simple design. It uses a triple-disc external occulting system, a single off axis multilayer coated mirror and a CCD camera. We present measurements of the EUV mirror roughness and reflectivity, tests of the image quality, and measurements of the stray light rejection performance. The mirror uses a novel multilayer design with three components that give HECOR a high throughput.

EUV reflectivity and stability of tri-component Al- based multilayers

We report on further development of three-material multilayer coatings made with a use of aluminum for the extreme ultra-violet (EUV) applications such as solar physics, high-order harmonic generation or synchrotron radiation. It was found that an introduction of refractory metal in Al-based periodic stack helps to reduce significantly an interfacial roughness and provides for a higher theoretical reflectance in the spectral range from 17 to 40 nm. The normal incidence reflectivity as high as 55 % at 17 nm, 50 % at 21 nm and 42 % at 30 nm was achieved with the new Al/Mo/SiC and Al/Mo/B4C multilayer mirrors, which have been optimized, fabricated and characterized with x-rays and synchrotron radiation. A good temporal and thermal stability of the tri-component Al-based multilayers has been observed over 3 years.

Design, conception, and metrology of EUV mirrors for aggressive environments

The development of new high power EUV sources and EUV space imaging requires optics having specific properties which depend on applications and operating conditions. These both applications are very different in the working multilayers environment. For the high power sources, multilayers are submitted to short pulses with high energy peak whereas, for the space imaging, multilayers are submitted to continuous flux with low level. Moreover photon energy and environment for both applications may be different. The environment may affect structure and top layer contamination when optics are stored, handled, mounted on the final device and finally operating. Main environmental parameters investigated are temperature and humidity variation. One objective is the optimisation of multilayer coatings to offer the highest resistance under photonic, ionic fluxes and temperature cycle. This means that interfacial diffusion between thin layers and degradation of the capping layers have to be avoided or reduced. The present study relies with designing, depositing and testing different structures of multilayer coatings in order to minimise the influence of the environment. Multilayer coatings based on molybdenum, silicon and silicon carbide materials have been deposited by magnetron sputtering on silicon and zerodur substrates. Samples were submitted to radiations emitted by an EUV source at wavelength closed to 13.5 nm. Furthermore they were also submitted to thermal cycles and annealing under warm humidity in the aim to simulate extremes storage or handling conditions as space missions conditions. The damages and the performance of the multilayers were evaluated by using grazing incidence reflectometry at 0.154 nm and EUV reflectometry at the operating wavelength. After a presentation of the multilayer design, deposition and metrology tools, we will describe the different environmental effects on the coatings to take in care during EUV source exposure, handling and storage conditions. First results on multilayers performances to EUV source exposure and space specification tests are presented. Main damages studies were on annealing, thermal cycling and warm humidity.

Development of multilayer coatings for Solar Orbiter EUV imaging telescopes

Since more than 20 years, Laboratoire Charles Fabry and Institut d’Astrophysique Spatiale are involved in development of the EUV multilayer coating for solar imaging. Previous instruments, such as the SOHO EIT and STEREO EUVI telescopes, employed the Mo/Si multilayer coatings, which offered at that time the best efficiency and stability. We present here recent results of the development of highly efficient EUV multilayers coatings at 17.4 nm and 30.4 nm for the Solar Orbiter mission. New multilayer structures, based on a combination of three materials including aluminum, have been optimized both theoretically and experimentally. We have succeeded to reduce interfacial roughness of Albased multilayers down to 0.5 nm via optimization of the multilayer design and the deposition process. The EUV peak reflectance of Al/Mo/SiC and Al/Mo/B4C multilayer coatings reaches 56% at 17.4 nm, the highest value reported up to now for this wavelength. We have also optimized specific bi-periodic structures that possess two reflection bands in the EUV range with high spectral selectivity. The EUV reflectivity of these Al-based dual-band coatings are compared with the Si/Mo/B4C baseline coating for Solar Orbiter. Since the stability of reflecting multilayer coating is an important issue for space missions, we have also studied the temporal stability as well as the resistivity of the coatings to thermal cycling and to proton irradiation. Experimental results confirm that Al/Mo/SiC and Al/Mo/B4C multilayer coatings are good candidates for the Solar Orbiter EUV imaging telescopes.

Experimental study of Cr∕Sc multilayer mirrors for the nitrogen Kα-emission line

The authors present an experimental study of Cr∕Sc multilayer mirrors optimized for the detection of the nitrogen Kα-emission line (λ=3.16nm) at a grazing incidence around 23°, for electron probe microanalysis applications. The multilayers were deposited onto silicon substrates using a dc magnetron sputtering system. They were characterized with grazing incidence copper Kα x-ray reflectometry and atomic force microscopy, as well as with at-wavelength reflectometry using synchrotron radiation. These various characterization methods pointed out that the interfacial roughness of these multilayers increases drastically with the number of bilayers. Growth parameters were then optimized, and it is shown that the structure and reflectivity of such multilayers can be considerably improved by optimizing the sputter gas pressure during the deposition process. Reflectivity higher than 37% were measured at 22.3° grazing angle for the nitrogen Kα-emission line.

X-ray broadband Ni/SiC multilayers: improvement with W barrier layers

We present an experimental study and performance improvement of periodic and aperiodic Ni/SiC multilayer coatings. Periodic Ni/SiC multilayer mirrors have been coated and characterized by grazing incidence X-ray reflectometry at 8.048 keV (Cu Kα radiation) and by measurements at 3 keV and 5 keV on synchrotron radiation facilities. An interdiffusion effect is found between Ni and SiC layers. A two-material model, Ni(x)Si(y)/SiC, using a silicide instead of Ni, was used to fit the measurements. The addition of 0.6 nm W barrier layers at the interfaces allows a significant reduction of the interdiffusion between Ni and SiC. In order to obtain a specific reflectivity profile in the 2 - 8 keV energy range, we have designed and coated aperiodic multilayer mirrors by using Ni/SiC with and without W barrier layers. The experimental reflectivity profiles as a function of the photon energy were measured on a synchrotron radiation facility in both cases. Adding W barrier layers in Ni/SiC multilayers provides a better precision on the layer thicknesses and a very good agreement between the experimental data and the targeted spectral profile.

Single and multi-channel Al-based multilayer systems for space applications in EUV range

We report on further development of reflective multilayer coatings containing aluminum as low absorbing material for the extreme ultra-violet (EUV) applications, in particular for solar physics. Optimizations of the multilayer design and deposition process have allowed us to produce Al-based multilayers having relatively low interface roughness and record EUV reflectances in the range from 17 to 40 nm. The peak reflectance values of 56 % at 17.5 nm, 50 % at around 21 nm, and 42 % at 32 nm were achieved with new three-material multilayers Al/Mo/SiC and Al/Mo/B4C at near-normal incidence. We observe a good temporal stability of optical parameters of the multilayers over the period of 4 years. Moreover, the multilayer structure remains stable upon annealing at 100 °C in air during several weeks. We will discuss the optical properties of more complex Al-based systems with regard to the design of multilayer coatings that reflect more than one wavelength and reject some others within the spectral range from 17 to 40 nm. Such multichannel systems with enhanced reflectance and selectivity would provide a further advance in optical performance and compactness of EUV solar imaging instruments. We will discuss general aspects of design, optimization and fabrication of single- and multi-channel multilayer mirrors made with the use of aluminum. We will present recent results on the EUV reflectivity of multilayer coatings based on the Al/Mo/SiC and Al/Mo/B4C material combinations. Al-based multilayer systems are proposed as optical coatings in EUV telescopes of future space missions and in other EUV applications.