Ger de Graaf

Compact gas cell integrated with a linear variable optical filter

A miniaturized methane (CH(4)) sensor based on nondispersive infrared absorption is realized in MEMS technology. A high level of functional integration is achieved by using the resonance cavity of a linear variable optical filter (LVOF) also as a gas absorption cell. For effective detection of methane at λ = 3.39 µm, an absorption path length of at least 5 mm is required. Miniaturization therefore necessitates the use of highly reflective mirrors and operation at the 15th-order mode with a resonator cavity length of 25.4 µm. The conventional description of the LVOF in terms of the Fabry-Perot resonator is inadequate for analyzing the optical performance at such demanding boundary conditions. We demonstrate that an approach employing the Fizeau resonator is more appropriate. Furthermore, the design and fabrication in a CMOS-compatible microfabrication technology are described and operation as a methane sensor is demonstrated.

Linear variable optical filter-based ultraviolet microspectrometer

An IC-compatible linear variable optical filter (LVOF) for application in the UV spectral range between 310 and 400 nm has been fabricated using resist reflow and an optimized dry-etching. The LVOF is mounted on the top of a commercially available CMOS camera to result in a UV microspectrometer. A special calibration technique has been employed that is based on an initial spectral measurement on a xenon lamp. The image recorded on the camera during calibration is used in a signal processing algorithm to reconstruct the spectrum of the mercury lamp and the calibration data is subsequently used in UV spectral measurements. Experiments on a fabricated LVOF-based microspectrometer with this calibration approach implemented reveal a spectral resolution of 0.5 nm.

High-resolution microspectrometer with an aberration-correcting planar grating

A concept for a highly miniaturized spectrometer featuring a two-component design is presented. The first component is a planar chip that integrates an input slit and aberration-correcting diffraction grating with an image sensor and is fabricated using microelectromechanical systems (MEMS) technologies. Due to the fabrication in a simple MEMS batch process the essential elements of the spectrometer are automatically aligned, and a low fabrication cost per device can be achieved. The second component is a spherical mirror, which is the only external part. The optimized grating structure compensates for aberrations within the spectrometer operating range, resulting in a diffraction-limited performance of the spectrometer optics. The prototype of the device has been fabricated and characterized. It takes a volume of 0.5 cm(3) and provides a FWHM spectral resolution of 0.7 nm over a 350 nm bandwidth from 420 nm to 770 nm combined with an etendue of 7.4x10(-5) mm(2) sr.

Spectral measurement using IC-compatible linear variable optical filter

This paper reports on the functional and spectral characterization of a microspectrometer based on a CMOS detector array covered by an IC-Compatible Linear Variable Optical Filter (LVOF). The Fabry-Perot LVOF is composed of 15 dielectric layers with a tapered middle cavity layer, which has been fabricated in an IC-Compatible process using resist reflow. A pattern of trenches is made in a resist layer by lithography and followed by a reflow step result in a smooth tapered resist layer. The lithography mask with the required pattern is designed by a simple geometrical model and FEM simulation of reflow process. The topography of the tapered resist layer is transferred into silicon dioxide layer by an optimized RIE process. The IC-compatible fabrication technique of such a LVOF, makes fabrication directly on a CMOS or CCD detector possible and would allow for high volume production of chip-size micro-spectrometers. The LVOF is designed to cover the 580 nm to 720 spectral range. The dimensions of the fabricated LVOF are 5×5 mm2. The LVOF is placed in front of detector chip of a commercial camera to enable characterization. An initial calibration is performed by projecting monochromatic light in the wavelength range of 580 nm to 720 nm on the LVOF and the camera. The wavelength of the monochromatic light is swept in 1 nm steps. The Illuminated stripe region on the camera detector moves as the wavelength is swept. Afterwards, a Neon lamp is used to validate the possibility of spectral measurement. The light from a Neon lamp is collimated and projected on the LVOF on the camera chip. After data acquisition a special algorithm is used to extract the spectrum of the Neon lamp.

Dielectric spectroscopy for measuring the composition of gasoline/water/ethanol mixtures

Dielectric spectroscopy is applied to investigate the feasibility of biofuel composition measurement. Measurements were made on the pure components (ethanol, gasoline and water) and mixtures thereof. Preliminary measurement results indicate that the components have distinguishable spectral dielectric behavior in the ranges 10-100 kHz and 200 MHz-2GHz. A simple linear-mixing algorithm is presented for calculating the composition from two different parameters of the measured data. Measurements show that ethanol concentration is relatively easy to determine by RF impedance measurements of the permittivity of the mixture, provided that the baseline is compensated for the water content. Unambiguous measurement of water content of different types of fuel at low frequencies is still hampered by the salinity of water and the presence of additives (static dissipaters) that lower the conductivity of gasoline.

Phase readout of thermal conductivity-based gas sensors

This work presents an integrated phase-domain ADC for surface-micromachined thermal-conductivity-based gas sensors. The concentration of hydrogen in air is detected via the concentration-dependent phase shift of an AC-driven thermal filter. Because thermal conductivity is measured in the phase, rather than in the amplitude domain, the readout circuit is insensitive to gain and offset errors. The ADC is implemented using a phase-domain sigma-delta modulator. Simulation results show that the system has a resolution of 0.06%rms H2 concentration in a 1Hz BW, while dissipating only 100µ;W in the thermal conductivity sensor.

Optical design and characterization of a gas filled MEMS Fabry-Perot filter

A concept for a highly integrated and miniaturized gas sensor based on infrared absorption, a Fabry-Perot type linear variable optical filter with integrated gas cell, is presented. The sample chamber takes up most of the space in a conventional spectrometer and is the only component that has so far not been miniaturized. In this concept the gas cell is combined with the resonator cavity of the filter. The optical design, fabrication, and characterization results on a MEMSbased realization are reported for a 24-25.5 μm long tapered resonator cavity. Multiple reflections from highly reflective mirrors enable this optical cavity to also act as a gas cell with an equivalent optical absorption path length of 8 mm. Wideband operation of the filter is ensured by fabrication of a tapered mirror. In addition to the functional integration and significant size reduction, the filter contains no moving parts, thus enables the fabrication of a robust microspectrometer

CMOS-compatible LVOF-based visible microspectrometer

This paper reports on a CMOS-Compatible Linear Variable Optical Filter (LVOF) visible micro-spectrometer. The CMOS-compatible post process for fabrication of the LVOF has been used for integration of the LVOF with a CMOS chip containing a 128-element photodiode array and readout circuitry. Fabrication of LVOF involves a process for fabrication of very small taper angles, ranging from 0.001° to 0.1°, in SiO2. These layers can be fabricated flexibly in a resist layer by just one lithography step and a subsequent reflow process. The 3D pattern of the resist structures is subsequently transferred into SiO2 by appropriate etching. Complete LVOF fabrication involves CMOS-compatible deposition of a lower dielectric mirror using a stack of dielectrics on the wafer, tapered layer formation and deposition of the top dielectric mirror. The LVOF has been optimized for 580 nm - 720 nm spectral operating range and has also been mounted on a CCD camera for characterization. The design of LVOF micro-spectrometer, the fabrication and characterization results are presented.

Analysis of the effect of stress-induced waviness in airgap-based optical filters

The preliminary results of a study on the effect of the membrane deformation on the optical response of the distributed Bragg reflector, that is based on a stack of such membranes, are presented. The analysis is applied to airgap-based optical filters, which offer an enhanced refractive index contrast and hence are highly promising for optical MEMS devices. The available methods and materials in MEMS technology would make fabrication of such devices feasible, but the optical requirements impose strict geometrical implications on the membrane structure. Although (an overall) tensile stress in membrane is expected to result in a flat structure after the release, a stress gradient results in a deformed structure. A combined finite element and finite-difference time- domain method has been utilized in this work to study the effects of a stress gradient in a distributed Bragg reflector. The results on the effects of both a linear and a non-linear stress gradient are presented. It is shown that a non-linear stress profile results in twice the deformation and a further reduction of optical performance.

Design and fabrication of ripple-free CMOS-compatible stacked membranes for airgap optical filters for UV-visible spectrum

CMOS-compatible fabrication of thin dielectric membranes for the ultraviolet and visible spectrum is presented for use in airgap/SiO 2 -based interference filter design. A typical optical design consists of multiple membranes of 50-100 nm thickness. Maintaining flatness over a large area, as required by the optical application, is challenging. In such a free-standing membrane, the residual stress is the main force acting on the structure. Although an overall tensile residual stress can effectively stretch the membrane, too much stress would exceed the yield strength of the material and results in fracturing. Furthermore, the presence of a residual stress gradient causes the membrane to deform. In this work, the effect of a stress profile in the thin film has is investigated. Although PECVD SiO 2 layers with an average tensile stress level of 178 MPa are used for the fabrication of the membranes, the presence of a stress gradient of about 0:67 MPa=nm results in a deformation in the membrane. A simple straining method is applied to reduce flatness. The preliminary results and discusses the challenges in the fabrication of stacked membranes for optical filters are presented.