Minseung Ahn

Fabrication of ultrahigh aspect ratio freestanding gratings on silicon-on-insulator wafers

The authors report a silicon-on-insulator (SOI) process for the fabrication of ultrahigh aspect ratio freestanding gratings for high efficiency x-ray and extreme ultraviolet spectroscopy. This new grating design will lead to blazed transmission gratings via total external reflection on the grating sidewalls for x rays incident at graze angles below their critical angle (about 1°–2°). This critical-angle transmission (CAT) grating combines the alignment and figure insensitivity of transmission gratings with high broadband diffraction efficiency, which traditionally has been the domain of blazed reflection gratings. The required straight and ultrahigh aspect ratio freestanding structures are achieved by anisotropic etching of ⟨110⟩ SOI wafers in potassium hydroxide (KOH) solution. To overcome structural weakness, chromium is patterned as a reactive ion etch mask to form a support mesh. The grating with period of 574nm is written by scanning-beam interference lithography (SBIL) which is based on the interfer...

A compact broadband tactile display and its effectiveness in the display of tactile form

This paper describes the development of a planar distributed tactile display, and tests its effectiveness for displaying textures. The tactile display is composed of a 6/spl times/5 pin array actuated by 30 piezoelectric bimorphs. The pins lie on 1.8 mm centers. Vertical excursion of each pin is controlled over a 0-0.7 mm range. Perceptual experiments were conducted to evaluate the performance of the system under three conditions: active touch, passive touch with vibration, and passive touch without vibration.

High-efficiency 5000 lines/mm multilayer-coated blazed grating for extreme ultraviolet wavelengths

Volume x-ray gratings consisting of a multilayer coating deposited on a blazed substrate can diffract with very high efficiency, even in high orders if diffraction conditions in-plane (grating) and out-of-plane (Bragg multilayer) are met simultaneously. This remarkable property, however, depends critically on the ability to create a structure with near atomic perfection. In this Letter we report on a method to produce these structures. We report measurements that show, for a 5000l/mm grating diffracting in the third order, a diffraction efficiency of 37.6% at a wavelength of 13.6nm. This work now shows a direct route to achieving high diffraction efficiency in high order at wavelengths throughout the soft x-ray energy range.

A compact planar distributed tactile display and effects of frequency on texture judgment

This paper describes the development of a planar distributed tactile display and the evaluation of the results of its effectiveness for displaying textures. The tactile display is composed of a 6 × 5 pin array actuated by 30 piezoelectric bimorphs. The distance between each pins centers is 1.8 mm. Vertical excursion of each pin is controlled over a 0–0.7 mm range. Perceptual experiments were conducted to evaluate the performance of the system under three conditions: active touch, passive touch with vibration and passive touch without vibration. The experimental results showed that vibrational stimuli helped subjects discriminate tactile patterns. Measurements of the error rate during discrimination tasks were used to find an optimal vibration frequency for stimuli presented at a constant sensation level (32 SLdB above threshold). The experiment was repeated, this time holding the energy transferred mechanically to the fingertip tissue constant. At low frequencies, we found that the passive stimulation allowed subjects to discriminate just as well as active touch of static stimuli did. The results suggested new possibilities for displaying texture using passive touch, constant energy and spatially varied vibration frequency.

Fabrication of 200nm period blazed transmission gratings on silicon-on-insulator wafers

The authors report on the fabrication of 200nm period blazed transmission gratings on silicon-on-insulator (SOI) wafers. These critical angle transmission (CAT) gratings require 3–5μm tall freestanding grating bars with a very high aspect ratio (>100) and smooth sidewalls. In order to meet the challenging geometrical requirements, they modified and improved our previously reported process for the fabrication of a CAT grating prototype with 574nm period. They have used potassium hydroxide (KOH) solutions to fabricate high aspect ratio gratings on ⟨110⟩ SOI wafers. The KOH etching process was improved to minimize the lateral undercut through precise grating alignment to ⟨111⟩ planes within ±0.05° and a room temperature etch process with 50wt% KOH. In addition, an image-reversal technique with a high silicon content spin-on polymer was applied to increase process latitude with a high duty cycle nitride mask. A surfactant was also added to the KOH solution to promote hydrogen bubble release. With the improved...

Blazed high-efficiency x-ray diffraction via transmission through arrays of nanometer-scale mirrors

Diffraction gratings are ubiquitous wavelength dispersive elements for photons as well as for subatomic particles, atoms, and large molecules. They serve as enabling devices for spectroscopy, microscopy, and interferometry in numerous applications across the physical sciences. Transmission gratings are required in applications that demand high alignment and figure error tolerances, low weight and size, or a straight-through zero-order beam. However, photons or particles are often strongly absorbed upon transmission, e.g., in the increasingly important extreme ultraviolet (EUV) and soft x-ray band, leading to low diffraction efficiency. We demonstrate the performance of a critical-angle transmission (CAT) grating in the EUV and soft x-ray band that for the first time combines the advantages of transmission gratings with the superior broadband efficiency of blazed reflection gratings via reflection from nanofabricated periodic arrays of atomically smooth nanometer-thin silicon mirrors at angles below the critical angle for total external reflection. The efficiency of the CAT grating design is not limited to photons, but also opens the door to new, sensitive, and compact experiments and applications in atom and neutron optics, as well as for the efficient diffraction of electrons, ions, or molecules.

Diffraction efficiency of 200-nm-period critical-angle transmission gratings in the soft x-ray and extreme ultraviolet wavelength bands

We report on measurements of the diffraction efficiency of 200-nm-period freestanding blazed transmission gratings for wavelengths in the 0.96 to 19.4 nm range. These critical-angle transmission (CAT) gratings achieve highly efficient blazing over a broad band via total external reflection off the sidewalls of smooth, tens of nanometer thin ultrahigh aspect-ratio silicon grating bars and thus combine the advantages of blazed x-ray reflection gratings with those of more conventional x-ray transmission gratings. Prototype gratings with maximum depths of 3.2 and 6 μm were investigated at two different blaze angles. In these initial CAT gratings the grating bars are monolithically connected to a cross support mesh that only leaves less than half of the grating area unobstructed. Because of our initial fabrication approach, the support mesh bars feature a strongly trapezoidal cross section that leads to varying CAT grating depths and partial absorption of diffracted orders. While theory predicts broadband absolute diffraction efficiencies as high as 60% for ideal CAT gratings without a support mesh, experimental results show efficiencies in the range of ∼50-100% of theoretical predictions when taking the effects of the support mesh into account. Future minimization of the support mesh therefore promises broadband CAT grating absolute diffraction efficiencies of 50% or higher.

High-efficiency multilayer blazed gratings for EUV and soft x-rays: recent developments

Multilayer coated blazed gratings with high groove density are the best candidates for use in high resolution EUV and soft x-ray spectroscopy. Theoretical analysis shows that such a grating can be potentially optimized for high dispersion and spectral resolution in a desired high diffraction order without significant loss of diffraction efficiency. In order to realize this potential, the grating fabrication process should provide a perfect triangular groove profile and an extremely smooth surface of the blazed facets. Here we report on recent progress achieved at the Advanced Light Source (ALS) in fabrication of high quality multilayer coated blazed gratings. The blazed gratings were fabricated using scanning beam interference lithography followed by wet anisotropic etching of silicon. A 200 nm period grating coated with a Mo/Si multilayer composed with 30 bi-layers demonstrated an absolute efficiency of 37.6% in the 3rd diffraction order at 13.6 nm wavelength. The groove profile of the grating was thoroughly characterized with atomic force microscopy before and after the multilayer deposition. The obtained metrology data were used for simulation of the grating efficiency with the vector electromagnetic PCGrate-6.1 code. The simulations showed that smoothing of the grating profile during the multilayer deposition is the main reason for efficiency losses compared to the theoretical maximum. Investigation of the grating with cross-sectional transmission electron microscopy revealed a complex evolution of the groove profile in the course of the multilayer deposition. Impact of the shadowing and smoothing processes on growth of the multilayer on the surface of the sawtooth substrate is discussed.

Fabrication and performance of blazed transmission gratings for x-ray astronomy

We have developed a new type of soft x-ray diffraction grating. This critical-angle transmission (CAT) grating combines the advantages of traditional transmission gratings (low mass, extremely relaxed alignment and flatness tolerances) with those of x-ray reflection gratings (high efficiency due to blazing in the direction of grazing-incidence reflection, increased resolution due to the use of higher diffraction orders). In addition, grating spectrometers based on CAT gratings are well-suited for co-existence with high-energy focal plane microcalorimeter detectors as planned for the Constellation-X mission, since most high-energy x rays are neither absorbed nor deflected, and arrive at the telescope focus. We describe the CAT grating principle and design, and fabrication and x-ray diffraction efficiency results for a CAT grating with 1742 lines/mm. We have observed up to 46% diffraction efficiency in a single order, and up to 55% at blaze at extreme ultraviolet wavelengths. We present our recent fabrication and soft x-ray diffraction results for 200 nm-period (5000 lines/mm) gratings.

5000 groove/mm multilayer-coated blazed grating with 33% efficiency in the 3rd order in the EUV wavelength range

We report on recent progress in developing diffraction gratings which can potentially provide extremely high spectral resolution of 105-106 in the EUV and soft x-ray photon energy ranges. Such a grating was fabricated by deposition of a multilayer on a substrate which consists of a 6-degree blazed grating with a high groove density. The fabrication of the substrate gratings was based on scanning interference lithography and anisotropic wet etch of silicon single crystals. The optimized fabrication process provided precise control of the grating periodicity, and the grating groove profile, together with very short anti-blazed facets, and near atomically smooth surface blazed facets. The blazed grating coated with 20 Mo/Si bilayers demonstrated a diffraction efficiency in the third order as high as 33% at an incidence angle of 11° and wavelength of 14.18 nm. This work was supported by the US Department of Energy under contract number DE-AC02-05CH11231.